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81.
82.
离子液体催化C_5馏分中二烯烃的聚合反应 总被引:1,自引:0,他引:1
合成了多种基于1-丁基-3-甲基咪唑阳离子的离子液体,并作为裂解C5馏分中混合二烯烃聚合反应的介质。考察了离子液体种类、反应温度、反应时间和添加Lew is酸对混合二烯烃聚合反应的影响。实验结果表明,以硝酸根为阴离子的离子液体对混合二烯烃的聚合反应具有一定的阻聚作用;以六氟磷酸根为阴离子的离子液体能明显促进混合二烯烃的聚合反应,提高二聚物的含量;添加Lew is酸(质量分数为1%的ZnCl2)的离子液体对混合二烯烃的聚合反应具有更明显的促进作用,其效果仅次于酸性氯铝酸类离子液体,反应温度以30℃以下为宜,温度过高将促使二聚物进一步聚合,形成三聚物乃至多聚物,降低二聚物的含量。 相似文献
83.
O. V. Konstantinova A. V. Kuz’mov V. V. Skorokhod M. B. Shtern 《Powder Metallurgy and Metal Ceramics》2007,46(1-2):25-31
A theoretical method for determining the percolation limit and effective conductivity of composites based on polydisperse
mixtures of insulator and conductor powders is proposed. The effect of the particle size ratio between the insulator and conductor
on the percolation limit and effective conductivity is studied. Numerical simulation of the microstructure, effective properties,
and percolation limit in composites is discussed.
__________
Translated from Poroshkovaya Metallurgiya, Vol. 46, No. 1–2(453), pp. 31–40, 2007. 相似文献
84.
Two macromodeling techniques using rational bases are investigated to accurately predict the natural frequencies of highly resonant microwave structures. Three methods are proposed and compared to calculate pole‐free solutions to the Thiele continued fraction and vector fitting pole‐residue models of the characteristic equation det[Z(s)]. © 2007 Wiley Periodicals, Inc. Int J RF and Microwave CAE, 2007. 相似文献
85.
86.
Besides equidistribution properties and statistical independence the lattice profile, a generalized version of Marsaglia's
lattice test, provides another quality measure for pseudorandom sequences over a (finite) field. It turned out that the lattice
profile is closely related with the linear complexity profile. In this article we give a survey of several features of the
linear complexity profile and the lattice profile, and we utilize relationships to completely describe the lattice profile
of a sequence over a finite field in terms of the continued fraction expansion of its generating function. Finally we describe
and construct sequences with a certain lattice profile, and introduce a further complexity measure. 相似文献
87.
A. Hammiche L. Bozec† H. M. Pollock M. German & M. Reading‡ 《Journal of microscopy》2004,213(2):129-134
Near‐field photothermal Fourier transform infra‐red microspectroscopy, which utilizes atomic force microscopy (AFM)‐type temperature sensors, is being developed with the aim of achieving a spatial resolution higher than the diffraction limit. Here we report on a new implementation of the technique. Sensitivity of the technique is assessed by recording infra‐red spectra from small quantities of analytes and thin films. A photothermomechanical approach, which utilizes conventional AFM probes as temperature sensors, is also discussed based on preliminary results. Early indication suggests that the photothermal approach is more sensitive than the thermomechanical one. 相似文献
88.
Henry D.I. Abarbanel Lev Korzinov Alistair I. Mees Igor M. Starobinets 《Systems & Control Letters》1997,31(5):820-276
Using optimal control techniques we derive and demonstrate the use of an explicit single-step control method for directing a nonlinear system to a target orbit and keeping it there. We require that control values remain near the uncontrolled settings. The full nonlinearity of the problem in state space variables is retained. The “one-step” of the control is typically a composition of known or learned maps over (a) the time required to learn the state, (b) the time to compute the control and (c) the time to apply the control. No special targeting is required, yet the time to control is quite rapid. Working with the dynamics of a well-studied nonlinear electrical circuit, we show how this method works efficiently and accurately in two situations: when the known circuit equations are used, and when control is performed only on a Poincaré section of the reconstructed phase space. In each case, because the control rule is known analytically, the control strategy is computationally efficient while retaining high accuracy. The target locations on the selected target trajectory at each control stage are determined dynamically by the initial conditions and the system dynamics, and the target trajectory is an approximation to an unstable periodic orbit of the uncontrolled system. A linear stability analysis shows that dissipation in the dynamical system is essential for reaching a controllable state. 相似文献
89.
90.
克拉玛依原油中各组分的乳化性质 总被引:3,自引:0,他引:3
用沉淀法和色谱分离法将克拉玛依原油分离成沥青质,极性物和抽余油三组分,红外光谱分析表明,沥青质和极性物中存在一些含氧官能团的羧酸类或酚类以及含氮化合物,而抽余油则主要为烃类物质,因而沥青质和极性物的界面活性大于抽余油,沥青质具有较强的油包水(W/O)乳化能力,是造成克拉玛依原油W/O乳化的主要组分,极性物具有较强的水包油(O/W)乳化能力,是造成克拉玛依原油O/W乳化的主要组分,抽余油的乳化能力很弱。 相似文献